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Abstract

Herbal cosmetics have gained significant popularity due to their minimal side effects, eco-friendly nature, and enhanced therapeutic benefits. Among these, herbal shampoos have emerged as a natural alternative to synthetic formulations that often contain harsh chemicals leading to scalp irritation and hair damage. This study focuses on the formulation and evaluation of a natural herbal shampoo using a blend of traditional medicinal plants known for their cleansing, conditioning, and restorative properties. Key ingredients include Cuscuta reflexa, Sapindus mukorossi (Reetha) all of which are recognized in Ayurveda for promoting hair health and treating scalp disorders. The herbal extracts were carefully selected based on their phytochemical profiles and synergistic actions. The formulation was evaluated for key physicochemical parameters such as pH, viscosity, foaming index, surface tension, wetting ability, and stability. It exhibited excellent cleansing properties, moderate foaming, good spreadability, making it suitable for regular use. Additionally, the presence of natural Bioactive imparts antimicrobial and antioxidant benefits, contributing to reduced dandruff, hair fall, and scalp irritation. The study concludes that the formulated herbal shampoo is a safe, effective, and sustainable alternative to commercial products. It holds promise for consumers seeking gentle, herbal-based hair care solutions and supports the integration of traditional knowledge with modern cosmetic science.

Keywords

Herbal shampoo , Cuscuta reflexa , Antimicrobial activity, Hair fall prevention

Introduction

Like common shampoo, herbal shampoo is a cosmetic product extracted from plant-based herbs that serves to clean the hair and scalp [1]. It serves as a substitute for the commercially sold synthetic shampoo [1]. Several medicinal herbs have been incorporated into shampoo formulas through history in efforts to improve hair health. Such therapeutic plants can be applied in the form of mixes, extracts, powders, or unprocessed forms. It is difficult to create a safer and gentler shampoo than supermarket shampoo using just one organic component [2]. Synthetic surfactants are added to synthetic shampoos mainly for their cleaning and foaming abilities, but long-term use of these surfactants has negative effects such as drying of the hair, irritation of the eyes, and scalp irritation [3]. The ideal characteristics of herbal shampoo are as follows:

  1. It should thoroughly and successfully cleanse the hair of loose corneal cells, excess sebum, or other fatty materials, as well as dust or dirt.
    2. It should generate a sufficient amount of foam to meet the user's psychological needs.
    3. Rinsing with water should make it easy to remove.
    4. The hair should be left non-dry, shiny, silky, manageable, and with little flyaway.
    5. It should give the hair a pleasing scent.
    6. It shouldn't irritate the skin or eyes or create any negative effects.

7. It shouldn't cause the hand to become rough and dry. [4]

Cuscuta: Cuscuta reflexa Roxb., Convolvulaceae family, is a leafless, twinning, parasitic dodder which is found on thin, elongated yellow stems that are profuse throughout tropical and temperate India. It's often called amarbel [5] Antitumor, antimicrobial, hepatoprotective, anticonvulsant, immunostimulatory, antioxidant, α-glucosidase inhibition,    Psychopharmacological, hair-growth-promoting, anti-steroidogenic, anti-inflammatory, diuretic, analgesic, antipyretic, anti-HIV, antidiabetic, neuroprotective, antiulcer, antispasmodi, heldynamic, bradycardia1, antihypertensive, cardiotonic, and muscle relaxant activities of various Cuscuta species were disclosed by pharmacological examination. [6]

Reetha: It belongs to a position to the Sapindaceae family and may be a massive deciduous tree with the rational name Sapindus mukorossi. It has common names that include aritha, dodan, dodani, soapberry, soapnut, and washnut.[7] Reetha is prepared from these dried natural product species, S. trifoliatus, which are members of the Sapindus family. Trifoliate II, hederagenin, oleanolic, saponin, sapindus corrosive, saponin A, and saponin B They are all sesquiterpenes. It is fair to use as a cleanser, astringent and soother. [8] Hair growth promoting action. The findings of the study depicted the possible anagen/telogen ratio, follicular density, and skin characteristics of Cuscuta reflexa extricate. Portion outcomes in relation to promoting hair growth. Perhaps the extricate has been enhanced. hair loss caused by androgen by inhibiting the conversion of testosterone dihydro testosterone to as indicated by the 5reductase movement is prevented by extricate and separate. [9] Because of its ability to create hair shining, firm, and sparkling, reetha is often utilized in typical hair care products. It is appropriate for regular use to support the hair scalp and stimulate hair growth. [10].

MATERIAL AND METHODS

Collection

All the required plant materials were collected from Nashik India's local market, and some were collected from Malegaon farms. The collected plant material was washed, dried, and powdered and stored for use in future experiments in an air-tight container. The Cascuta plant was washed with running water to remove impurities. The plant was dried in the sun, coarsely powdered, and then was exposed to extraction via decoction. After decoction, it was left to stand for 24 hours. The remaining material was pressed and filtered out. Boil the Reetha powder in a specified amount of water for 30 mins, reduce the volume to 1/4th of the original, cool the mixture and then filter For approximately ten minutes, flaxseeds boil with water by stirring continuously to avoid the flaxseeds sticking to the bottom of the utensil. When the consistency is gel-like and not too thin or too thick, switch off the stove. Let the gel cool for about one hour so that it can thicken.

Preparation of Shampoo

The formula given in the table can be employed to prepare the herbal shampoo using the primary emulsion method. The water phase consists of methyl paraben, glycerine, and polyethylene glycol (PEG), whereas the oil phase consists of caster oil and herb extract. Mix the extracts, water phase, and oil phase with constant stirring. Acacia and tragacanth facilitate the creation of an oil-in-water (o/w) emulsion. Then, use glycerine and PEG 400 to bring the volume to 100 ml. Add sufficient 1% citric acid solution to the solution to make its pH adjustable. add a few drops of perfume judiciously to give fragrance. [11]

Experimental work

Table 1: Shampoo Batches

Sr. No

Ingredients

F1

[100ml]

F2

[100ml]

F3

[100ml]

F4

[100ml]

F5

[100ml]

1.

CuscutaExtract

25ml

25ml

25ml

20ml

25ml

2.

Reetha extract

25ml

15ml

25ml

10ml

30ml

3.

Caster Oil

3gm

7gm

5gm

10gm

5gm

4.

Polyethylene Glycol

10ml

15ml

8ml

10ml

6ml

5.

Glycerin

3gm

5gm

2gm

10gm

5gm

6.

Methyl Paraben

4gm

3gm

6gm

4gm

3gm

7.

Acacia

5gm

5gm

7gm

8gm

3gm

8.

Tragacanth

5gm

5gm

7gm

8gm

3gm

9.

Flaxseed extract

20ml

20ml

15ml

20ml

20ml

10.

Essential Oil

qs

qs

qs

qs

qs

11.

Citric Acid Solution

qs

qs

qs

qs

qs

Step 1: Plant dried and converted into powder

Reference

  1. Sekar M. Formulation and evaluation of herbal shampoo containing rambutan leaves extract. Int J Pharm Bio Sci. Oct 2016.
  2. Telrandhe U, Sheikh NAW. Formulation, evaluation and comparison of herbal shampoo with commercially available shampoo. ResearchGate. Oct 2023.
  3. Bhavani MS, Jan SM, Rani KS, Srirekha M. Formulation, evaluation and composition of the herbal shampoo with commercial shampoo. Int J Pharm Sci Rev Res. Jan 15, 2023.
  4. Maurya P, Maurya S, Yadav P, Yadav MK, Maurya S, Jaysawal S. A review article on herbal shampoo. JETIR. May 2021;8(5).
  5. Patel S, Sharma V, Chauhan NS, Dixit VK. A study on the extracts of Cuscuta reflexa Roxb. in treatment of cyclophosphamide induced alopecia. DARU J Pharm Sci. 2014; 22:7.
  6. Saini P, Mithal R, Menghani E. A parasitic medicinal plant Cuscuta reflexa: An overview. Int J Sci Eng Res. Dec 2015;6(12):951.
  7. Sharma A, Virk S. The Pharmaceutical and Chemical Journal. 2023;10(4):20-29.
  8. Sbhatu DB, Berhe GG, Hndeya AG, Abraha HB, Abdu A, Gebru HA, Taye MG, Mulugeta A, Weldemichael MY, Tekle HT, Kidanemariam HG. Formulation and physicochemical evaluation of lab-based Aloe adigratana Reynolds shampoos. Int J Anal Chem. 2020; Article ID 6290617:7 pages.
  9. Chishti MA, Akram M, Ozdemir FA, Ghauri AO, Sfera A, Parmar P. Cuscuta reflexa traditional miracle plant: A review on ethnomedicinal and therapeutic potential. Int Arch Integr Med. 2024;11(1):1-8.
  10. Sayyad TR, Chaudhari SS, Nikumbh PP, Bhurat MR. Evaluation, composition and comparative study of hair growing tonic. Pharm Resonance. 2023;6(1):12.
  11. Shinde VM, Bodas YKS. A practical book of herbal drug technology. 3rd ed. Nirali Publication; July 2023.
  12. Vijayalakshmi A, Sangeetha S, Ranjith N. Formulation and evaluation of herbal shampoo. 2018;11(Special Issue 4).
  13. Arora R, Singh RK, Bharakatiya M. Formulation and evaluation of herbal shampoo by extract of some plants. Pharm Chem J. 2019;6(4):74-80.
  14. AlQuadeib BT, Eltahir EKD, Banafa RA, Al-Hadhairi LA. Pharmaceutical evaluation of different shampoo brands in local Saudi market. [Details incomplete].
  15. Preethi PJ, Padmini K, Srikanth J, Lohita M, Swetha K, Rao PV. A review on herbal shampoo and its evaluation. Asian J Pharm Anal. 2013;3(4):153-156.
  16. Namita, Nimisha. Formulation and evaluation of herbal shampoo having antimicrobial potential. Int J Pharm Pharm Sci. 2013; 5:708-12.
  17. Waghmode MV, Hingane LD. Formulation and evaluation of herbal shampoo. Int J Res Appl Sci Eng Technol (IJRASET). 2022;10(6).
  18. Dilli Prasad KM, et al. Preparation and evaluation of herbal shampoo. Int J Indigenous Herbs Drugs. 2024:8-12.
  19. Reddy KV, Yachawad AV, Zambare KK, Landge S. Formulation and evaluation of herbal shampoo: Bryophyllum pinnatum. 2020;10(2).
  20. Noureen S, et al. The genus Cuscuta (Convolvulaceae): An updated review on indigenous uses, phytochemistry, and pharmacology. Iran J Basic Med Sci. 2019;22(11):1225.

Photo
Harshal Shewale
Corresponding author

Pharmacology Department MET institute of D Pharmacy, Adgaon

Photo
Nikita Nagare
Co-author

Pharmacology Department MET institute of D Pharmacy, Adgaon

Photo
Bhavesh Salunke
Co-author

Pharmacology Department MET institute of D Pharmacy, Adgaon

Photo
Hemant Raut
Co-author

Pharmacology Department MET institute of D Pharmacy, Adgaon

Photo
MRN. Shaikh
Co-author

Pharmacology Department MET institute of D Pharmacy, Adgaon

Harshal Shewale*, Nikita Nagare, Bhavesh Salunke, Hemant Raut, MRN. Shaikh, Development and Characterization of Herbal Shampoo from Cuscuta Reflexa, Int. J. Sci. R. Tech., 2025, 2 (4), 502-509. https://doi.org/10.5281/zenodo.15257535

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